Monday, 25 December 2023

Soap in Textile Wet processingSoap in Textile Wet processing

 

Soaps:  
  •            Soaps are sodium or potassium salts of higher fatty acids (are organic acids that have carbon atoms within 9-17 in their molecules) like stearic, palmitic and oleic acids.  
  •       Soap is a metallic salt of saturated (CnH2n+1COOH) or unsaturated (CnH2n-1COOH) higher fatty acid.
  •      There may be Pb, Mg, Ca or other metallic salts.  
  •      The sodium soaps are called hard soaps and The potassium soaps are known as soft soaps.
  •      Soaps are obtained from oils and fats.
  •       For example, tri-stearin is got from beef and mutton tallow, tri-palmitin from palm oil and tri-olein from lard (pig fat), olive oil and cotton seed oil.


Properties of soaps:
1. Soap dissolves very slowly in cold water but rapidly in hot water.
2. Soap dissolves in hot alcohol but is only carefully soluble in other organic solvents such as acetone, ether or petroleum.
3. Sometimes there are free fatty acid molecules in soap to form what is known as acid soaps.
4. Soap reacts with hard water to form insoluble soap.
5.  The number of carbon atoms in the aliphatic chain of soap is very important.
  
  The number of carbon atoms (C) < 9 : No detergency power  
  The number of carbon atoms within (C) 9-17 : Extremely good detergent
  The number of carbon atoms (C) 17 : Poor solubility

Cleansing action of soap:
Soap has two dissimilar ends. At one end it has the hydrocarbon chain that is non-polar and hydrophobic (soluble in oil/dirt). At the other end there is the carboxylate ion that is polar and hydrophilic (water soluble). When soap is added to water, its molecules make a unimolecular film on the surface of water with their carboxyl groups dissolved in water and the hydrocarbon chains standing on end to form a hydrocarbon layer. When a dirty cloth is soaked into a soap solution, soap dissolves fat or oil with dust by micelle formation. 



The fat or oil with dust is dissolved in water by hydrophobic hydrocarbon chains of soap. The water soluble carboxylate ions make a hydrophilic surface in water and render the micelles of oil or fat from the cloth to the water. Thus, the micelle is dissolved in water and is washed away. Soap tends to concentrate on the solution surface and therefore lowers its surface tension, causing foaming. This helps it to penetrate the fabric. It emulsifies fat and dirt to form micelles and make all the micelles water-soluble. Thus, the water washes the dirt away.




The structure of a micelle



The hydrophobic tails ‘burrow’ into the droplet of oil or grease. The hydrophilic heads are left to face the surrounding water. This results in the formation of a ball-like structure (a micelle).

Saponification:
 In simple terms, saponification is the name for a chemical reaction between an acid and a base to form a salt.
The vegetable oil is a glyceride of fatty acid (Oleic, stearic, palmitic acid), which is immiscible with water.  
When such oil is heated with a solution of sodium hydroxide in water, the oil is split into fatty acid and glycerine.  
This fatty acid reacts with sodium hydroxide solution and form sodium salt like soap which is soluble in water.  
This reaction is called saponification. As a result of saponification, the insoluble and water immiscible oil is converted to water soluble products.

SOAP  
  Soaps are sodium or potassium salts of long chain fatty acids.
  When triglycerides in fat/oil react with aqueous NaOH or KOH, they are converted into soap and glycerol.  

  This is called alkaline hydrolysis of esters. Since this reaction leads to the formation of soap, it is called the Saponification process.

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